Contents

Agilent 1260 Infinity II Low Dispersion Kit Technical Note PDF

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Summary of Content for Agilent 1260 Infinity II Low Dispersion Kit Technical Note PDF

1260 Infinity II Low Dispersion Kit

Technical Note

This note describes how to install the 1260 Infinity II Low Dispersion Kit (G7111-68708) and 1260 Infinity II Bio Low Dispersion Kit (G7131-68708).

Delivery Checklist 2

Installation 3

Install the Heat Exchanger Assembly 3 Install the Column 7

Delivery Checklist

Delivery Checklist G7111-68708:

G7131-68708:

p/n Description

5500-1201 Capillary ST 0.12 mm x 105 mm SL Heat exchanger to column

5500-1157 Capillary ST 0.12 mm x 500 mm SL/S Sampler to heat exchanger

G7116-60015 Quick Connect Heat Exchanger Standard

G7167-68703 Fitting Intermediate Kit

p/n Description

5500-1593 Quick Turn Capillary MP35N 0.12 mm x 105 mm Heat exchanger to column

5500-1279 Capillary MP35N 0.12 mm x 500 mm SI/SI Sampler to heat exchanger

G7116-60071 Quick Connect Bio Heat Exchanger Standard Flow

5067-5966 InfinityLab Quick Turn Fitting

2

Installation

Installation

Install the Heat Exchanger Assembly

Tools required p/n Description 8710-0510 Open-end wrench 1/4 5/16 inch

Parts required p/n Description The following parts are suitable for the 1260 Infinity II LC:

5500-1201 Capillary ST 0.12 mm x 105 mm SL

5500-1157 Capillary ST 0.12 mm x 500 mm SL/S

G7116-60015 Quick Connect Heat Exchanger Standard

G7167-68703 Fitting Intermediate Kit

The following parts are suitable for the 1260 Infinity II Prime Bio LC:

5500-1593 Quick Turn Capillary MP35N 0.12 mm x 105 mm

5500-1279 Capillary MP35N 0.12 mm x 500 mm SI/SI

G7116-60071 Quick Connect Bio Heat Exchanger Standard Flow

5067-5966 InfinityLab Quick Turn Fitting

3

Installation

CAUTION Excessive torque applied to the port of the Quick Connect Heat Exchanger can damage it.

Do not apply excessive torque to the heat exchanger port.

Always use a wrench to counter the heat exchanger port while tightening the capillary fitting.

NOTE Do not mix capillaries dedicated for different systems.

Low dispersion capillaries suitable for 1260 Infinity II LC system are marked by red sleeves.

Bio low dispersion capillaries suitable for 1260 Infinity II Prime Bio LC system are marked by red sleeves with an orange stripe.

NOTE Follow the special instructions provided for the Quick Connect and Quick Turn Fittings.

4

Installation

1 Choose one of the possible positions for placing the heat exchanger.

2 Connect the sampler outlet capillary 0.12 mm x 500 mm from port 6 of the sampler injection valve to the inlet port of the heat exchanger.

3 Connect the column connection capillary 0.12 mm x 105 mm to the outlet of the Quick Connect Heat Exchanger.

NOTE Use one of the four central positions if only one column is used.

Max. 2.5 Nm

Max. 2.5 Nm

5

Installation

4 Position the heat exchanger in the groove of the MCT heater block and prepare column holders to fix the heat exchanger.

5 Turn column holders to fix the Quick Connect Heat Exchanger in the MCT.

6

Installation

Install the Column

Tools required p/n Description

8710-0510 Open-end wrench 1/4 5/16 inch

Parts required p/n Description

The following parts are suitable for the 1260 Infinity II LC:

5500-1201 Capillary ST 0.12 mm x 105 mm SL

G7167-68703 Fitting Intermediate Kit

The following parts are suitable for the 1260 Infinity II Prime Bio LC:

5500-1593 Quick Turn Capillary MP35N 0.12 mm x 105 mm

5067-5966 InfinityLab Quick Turn Fitting

Preparations Capillary ST 0.12 mm x 105 mm SL (5500-1201) or Quick Turn Capillary MP35N 0.12 mm x 105 mm (5500-1593) connected to the heat exchanger, see Install the Heat Exchanger Assembly on page 3.

NOTE Do not mix capillaries dedicated for different systems.

Low dispersion capillaries suitable for 1260 Infinity II LC system are marked by red sleeves.

Bio low dispersion capillaries suitable for 1260 Infinity II Prime Bio LC system are marked by red sleeves with an orange stripe.

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1 Connect capillary 0.12 mm x 105 mm from the heat exchanger to the column.

2 Install capillary between the column and the detector flow cell (Quick Turn fitting to the column).

3 Position the column into the column holder clips.

NOTE After using the system with high salt concentrations, flush it extensively with water to prevent blockages caused by salt crystals. Regular extensive washes with water are mandatory when using LD capillaries.

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